Article

Cpd-A1 alleviates acute kidney injury by inhibiting ferroptosis

Ying Chen1, Ming-fei Wu2, Man-man Xie1, Yang Lu2, Chao Li1, Shuai-shuai Xie1, Wen-xian Ma1, Ming-lu Ji1, Rui Hou1, Ze-hui Dong3, Ruo-bing He1, Meng-meng Zhang1, Hao Lu1, Li Gao4, Jia-gen Wen1, Juan Jin5, Xiao-wu Dong2, Jin-xin Che2, Xiao-ming Meng1
1 Inflammation and Immune Mediated Diseases Laboratory of Anhui Province, the Key Laboratory of Anti-inflammatory of Immune Medicines, Ministry of Education, Anhui Institute of Innovative Drugs, School of Pharmacy, Anhui Medical University, Hefei 230032, China
2 Hangzhou Institute of Innovative Medicine, Institute of Drug Discovery and Design, College of Pharmaceutical Sciences, Zhejiang University, Hangzhou 310058, China
3 Department of Pharmacy, The Second Affiliated Hospital of Anhui University of Traditional Chinese Medicine, Hefei 230061, China
4 Department of Nephropathy, The First Affiliated Hospital of Anhui Medical University, Hefei 230022, China
5 School of Basic Medicine, Anhui Medical University, Hefei 230032, China
Correspondence to: Jin-xin Che: chejx@zju.edu.cn, Xiao-ming Meng: mengxiaoming@ahmu.edu.cn,
DOI: 10.1038/s41401-024-01277-w
Received: 18 November 2023
Accepted: 25 March 2024
Advance online: 19 April 2024

Abstract

Acute kidney injury (AKI) is defined as sudden loss of renal function characterized by increased serum creatinine levels and reduced urinary output with a duration of 7 days. Ferroptosis, an iron-dependent regulated necrotic pathway, has been implicated in the progression of AKI, while ferrostatin-1 (Fer-1), a selective inhibitor of ferroptosis, inhibited renal damage, oxidative stress and tubular cell death in AKI mouse models. However, the clinical translation of Fer-1 is limited due to its lack of efficacy and metabolic instability. In this study we designed and synthesized four Fer-1 analogs (Cpd-A1, Cpd-B1, Cpd-B2, Cpd-B3) with superior plasma stability, and evaluated their therapeutic potential in the treatment of AKI. Compared with Fer-1, all the four analogs displayed a higher distribution in mouse renal tissue in a pharmacokinetic assay and a more effective ferroptosis inhibition in erastin-treated mouse tubular epithelial cells (mTECs) with Cpd-A1 (N-methyl-substituted-tetrazole-Fer-1 analog) being the most efficacious one. In hypoxia/reoxygenation (H/R)- or LPS-treated mTECs, treatment with Cpd-A1 (0.25 μM) effectively attenuated cell damage, reduced inflammatory responses, and inhibited ferroptosis. In ischemia/reperfusion (I/R)- or cecal ligation and puncture (CLP)-induced AKI mouse models, pre-injection of Cpd-A1 (1.25, 2.5, 5 mg·kg−1·d−1, i.p.) dose-dependently improved kidney function, mitigated renal tubular injury, and abrogated inflammation. We conclude that Cpd-A1 may serve as a promising therapeutic agent for the treatment of AKI.

Keywords: AKI; ferroptosis; ferrostatin-1; Cpd-A1; tissue distribution; lipid peroxidation

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